10.14489/td.2015.07.pp.050-053

2015, 07 July

DOI: 10.14489/td.2015.07.pp.050-053

Livshits A. M., Gorskii E. V.
ELECTRO-CONTACT SAMPLING FOR THE ANALYSIS OF HIGH-ALLOY STEELS USING OPTICAL EMISSION SPECTROMETER PAPUAS-4
(pp. 50-53)

Abstract. It is presented a method of electro-contact sampling for optical emission spectral analysis of high-alloy steels. The advantage of this sampling is a possibility to study bulky samples without any need to cut the fragments for the analysis. It is shown that this method allows measuring elements contents without substantial degrading of measurement accuracy and repeatability. It is also shown that matrix effects for some elements are smaller than in case of analysis of bulk samples.

Keywords: sampling, sample preparation, optical emission spectroscopy (OES), high-alloy steel, alloys analysis, atomic spectroscopy, matrix effects, chemometrics, regression analysis.

+ - About the Authors Click to collapse

А. M. Livshits
Institute for Spectroscopy RAS, Troitsk, Moscow, Russia.

E. V. Gorskii
Ltd. “NPO “Spectropripor”, Moscow Region, Podolsk, Russia. E-mail: Данный адрес e-mail защищен от спам-ботов, Вам необходимо включить Javascript для его просмотра.

+ - References Click to collapse

1. Buravlev Iu. M. (2000). Atomic emission spectrome-try of metals and alloys. Donetsk: DonNU.
2. Thomsen V. B. E. (1996). Modern spectrochemical analysis of metals. ASM International.
3. Taganov K. I. (1968). Spectral analysis of metals and alloys with preliminary sampling. Moscow: Metallurgia.
4. Gorskii E. V., Livshits A. M., Mavrin N. B. (2010). Application of contact and impulse sample taking in emis-sion spectral analysis of titanium alloys. Kontrol'. Diagnostika, (11).
5. Buravlev Iu. M. (1970). The influence of composi-tion and sample size on the results of spectral analysis of alloys. Kiev: Tekhnika.
6. Gorskii E. V., Livshits A. M., Peleznev A. V. (2006). Determing the influence of the «third» elements in the analysis of aluminum alloys in emission spectrometer «PAPUAS-4». Zavodskaia laboratoriia, (3).

+ - Purchase digital version of a single article Click to collapse

This article is available in electronic format (PDF).

DOI: 10.14489/td.2015.07.pp.050-053

Copy the article DOI and follow the link https://id-spektr.ru/product/pokupka-elektronnoy-stati-iz-zhurnala-kontrol-diagnostika

Please specify the article DOI in the order comments.